
Brookeld Engineering Labs., Inc. Page 81 Manual No. M03-165-F0612
Calibration Procedure for a Small Sample Adapter
Brookeldrecommendsatwostepcheck.Firstverifythecalibrationoftheviscometerusingthe
standard viscometer spindles (LV #1-3, RV #2-6, HA #2-6 and HB #2-6 or cone/plate spindles) as
detailed in this appendix. Second verify the calibration of the viscometer using the Small Sample
Adapter. The use of an accessory device may increase the accuracy of measurement associated
with the DV-II+Pro.
When a Small Sample Adapter is used, the water jacket is connected to the water bath and the
waterisstabilizedatthepropertemperature:
1) Puttheproperamountofviscositystandarduidintothesamplechamber.Theamountvaries
with each spindle/chamber combination. (Refer to the Small Sample Adapter instruction
manual).
2) Place the sample chamber into the water jacket.
3) Putthespindleintothetestuidandattachtheextensionlink,couplingnutandfreehanging
spindle (or directly attach the solid shaft spindle) to the DV-II+Pro.
4) Allow 30 minutes for the viscosity standard, sample chamber and spindle to reach test temperature.
5) Measure the viscosity and record the Viscometer reading.
Note: The spindle must rotate at
least ve (5) times before readings are taken.
Calibration Procedure for a Thermosel System
Brookeldrecommendsatwostepcheck.Firstverifythecalibrationoftheviscometerusingthe
standard viscometer spindles (LV #1-3, RV #2-6, HA #2-6 and HB #2-6 or cone/plate spindles) as
detailed in this appendix. Second verify the calibration of the viscometer using the Thermosel.
The use of an accessory device may increase the accuracy of measurement associated with the
DV-II+Pro.
When a Thermosel System is used, the controller stabilizes the Thermo Container at the test
temperature.
1) Put theproper amountof HTviscosity standarduid intotheHT-2samplechamber.The
amount varies with the spindle used. (Refer to the Thermosel instruction manual).
2) Place the sample chamber into the Thermo Container.
3) Putthespindleintothetestuidandattachtheextensionlink,couplingnutandfreehanging
spindle (or directly attach the solid shaft spindle) to the DV-II+Pro.
4) Allow 30 minutes for the viscosity standard, sample chamber and spindle to reach test temperature.
5) Measure the viscosity and record the Viscometer reading.
Note: The spindle must rotate at
least ve (5) times before readings are taken.
Calibration Procedure using UL or DIN Adapters
Brookeldrecommendsatwostepcheck.Firstverifythecalibrationoftheviscometerusingthe
standard viscometer spindles (LV #1-3, RV #2-6, HA #2-6 and HB #2-6 or cone/plate spindles)
as detailed in this appendix. Second verify the calibration of the viscometer using the UL or DIN
Adapters. The use of an accessory device may increase the accuracy of measurement associated
with the DV-II+Pro.
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